and you can shake the crap out of it to collide really well. If one's aqueous is basified really well then there will not be any problems at all with seperation. the extra heat will yes allow the NP to be able to solute alittle more spice but also it will allow other impurities to make it into the NP, resulting in a less pure product. I believe in his tek he uses a hot water to speed up seperation of the NP. however if you dont use to much naptha to begin with, this wont be a problem. The main thing with freeze precip is that the Naptha needs to be somewhat saturated in order to precip ALL the alks.Īfter one does all there naptha pulls, they can combine them then evap until the naptha looks cloudy or when you see spice sticking to the bottom (thus you know it's completly saturated). You can do it in anything just about (as long as it's sealed). stay tuned for a pictorial of the process. My friend is almost done with his a/b doing everything mentioned here and then some, I finally convinced him to take pictures along the way. One can convert N-oxide to regular dm using a reducing agent, however if your going to go that route I would do an a/b and do the reaction in the main aqeuous before basifying as a ph of 3 is needed for the reaction. filter then proceed to a freeze precip on the naptha. you can keep it like this to have what we call jungle or you could dump it into some naptha (minimul as possible), the spice will disolve but the other alks and n-oxide will not. there will be more alks and n-oxide present. you wont be able to freeze precip these however.

I dont believe all the cell walls get broken down asap.Īfter you have exauhsted your basified slurry with naptha then do a couple of pulls with either xylene, tuolene, or d-limonene. These numbers are are an estimate to my own experience. A stb doesnt leave you with many options other then allow the mhrb to soak in the basified solution for a while, which does help.įrom my experiments with stb I found that near 90% would free base just letting sit like 3 hours or so, for the other 10% days.,

High yield dmt tek